PXRD Data 2θ (°) I (count) σ (count) PXRD Experimental Details 10.000 0 0.0 Title Heat treated hydroxyapatite N4660. 10.050 2 1.4 Filename D04763 10.100 3 1.7 Date and time 14-Sep-2016 at 11:24:37 10.150 0 0.0 Instrument Siemens D500 10.200 0 0.0 Sample type Flat-plate 10.250 0 0.0 X-ray radiation Cu Kα1 (using 40kV and 30mA) 10.300 0 0.0 Wavelength (in Å) 1.54056 10.350 3 1.7 2θ scan range: 1 10.000° to 55.000° step 0.050° at 4.0 s/step 10.400 1 1.0 Data treatment None 10.450 0 0.0 10.500 1 1.0 10.550 2 1.4 10.600 5 2.2 10.650 1 1.0 10.700 2 1.4 10.750 1 1.0 10.800 18 4.2 10.850 22 4.7 10.900 16 4.0 10.950 4 2.0 11.000 1 1.0 11.050 2 1.4 11.100 0 0.0 11.150 1 1.0 11.200 1 1.0 11.250 1 1.0 11.300 2 1.4 11.350 0 0.0 11.400 0 0.0 11.450 0 0.0 11.500 1 1.0 11.550 1 1.0 11.600 1 1.0 11.650 3 1.7 11.700 0 0.0 11.750 2 1.4 11.800 1 1.0 11.850 0 0.0 11.900 0 0.0 11.950 0 0.0 12.000 0 0.0 12.050 0 0.0 12.100 1 1.0 12.150 3 1.7 12.200 1 1.0 12.250 0 0.0 12.300 0 0.0 12.350 1 1.0 12.400 0 0.0 12.450 0 0.0 12.500 0 0.0 12.550 0 0.0 12.600 0 0.0 12.650 0 0.0 12.700 1 1.0 12.750 1 1.0 12.800 0 0.0 12.850 1 1.0 12.900 1 1.0 12.950 0 0.0 13.000 0 0.0 13.050 3 1.7 13.100 0 0.0 13.150 1 1.0 13.200 3 1.7 13.250 1 1.0 13.300 3 1.7 13.350 0 0.0 13.400 0 0.0 13.450 0 0.0 13.500 0 0.0 13.550 1 1.0 13.600 1 1.0 13.650 6 2.4 13.700 0 0.0 13.750 0 0.0 13.800 0 0.0 13.850 0 0.0 13.900 1 1.0 13.950 2 1.4 14.000 0 0.0 14.050 1 1.0 14.100 0 0.0 14.150 0 0.0 14.200 1 1.0 14.250 0 0.0 14.300 1 1.0 14.350 1 1.0 14.400 0 0.0 14.450 0 0.0 14.500 3 1.7 14.550 0 0.0 14.600 2 1.4 14.650 0 0.0 14.700 0 0.0 14.750 0 0.0 14.800 1 1.0 14.850 1 1.0 14.900 0 0.0 14.950 0 0.0 15.000 0 0.0 15.050 1 1.0 15.100 0 0.0 15.150 1 1.0 15.200 0 0.0 15.250 2 1.4 15.300 0 0.0 15.350 0 0.0 15.400 0 0.0 15.450 3 1.7 15.500 0 0.0 15.550 0 0.0 15.600 0 0.0 15.650 1 1.0 15.700 0 0.0 15.750 1 1.0 15.800 1 1.0 15.850 1 1.0 15.900 1 1.0 15.950 3 1.7 16.000 1 1.0 16.050 1 1.0 16.100 0 0.0 16.150 4 2.0 16.200 1 1.0 16.250 1 1.0 16.300 0 0.0 16.350 1 1.0 16.400 0 0.0 16.450 0 0.0 16.500 0 0.0 16.550 0 0.0 16.600 0 0.0 16.650 1 1.0 16.700 0 0.0 16.750 1 1.0 16.800 4 2.0 16.850 1 1.0 16.900 10 3.2 16.950 3 1.7 17.000 0 0.0 17.050 0 0.0 17.100 0 0.0 17.150 0 0.0 17.200 0 0.0 17.250 0 0.0 17.300 2 1.4 17.350 0 0.0 17.400 0 0.0 17.450 0 0.0 17.500 2 1.4 17.550 0 0.0 17.600 0 0.0 17.650 1 1.0 17.700 0 0.0 17.750 0 0.0 17.800 0 0.0 17.850 0 0.0 17.900 1 1.0 17.950 0 0.0 18.000 0 0.0 18.050 1 1.0 18.100 1 1.0 18.150 0 0.0 18.200 0 0.0 18.250 0 0.0 18.300 2 1.4 18.350 0 0.0 18.400 1 1.0 18.450 0 0.0 18.500 0 0.0 18.550 0 0.0 18.600 0 0.0 18.650 0 0.0 18.700 0 0.0 18.750 0 0.0 18.800 3 1.7 18.850 6 2.4 18.900 1 1.0 18.950 2 1.4 19.000 0 0.0 19.050 0 0.0 19.100 1 1.0 19.150 1 1.0 19.200 0 0.0 19.250 0 0.0 19.300 0 0.0 19.350 1 1.0 19.400 0 0.0 19.450 0 0.0 19.500 0 0.0 19.550 0 0.0 19.600 0 0.0 19.650 4 2.0 19.700 0 0.0 19.750 0 0.0 19.800 0 0.0 19.850 0 0.0 19.900 1 1.0 19.950 0 0.0 20.000 0 0.0 20.050 0 0.0 20.100 0 0.0 20.150 0 0.0 20.200 2 1.4 20.250 0 0.0 20.300 0 0.0 20.350 1 1.0 20.400 0 0.0 20.450 3 1.7 20.500 0 0.0 20.550 0 0.0 20.600 0 0.0 20.650 1 1.0 20.700 1 1.0 20.750 0 0.0 20.800 2 1.4 20.850 0 0.0 20.900 0 0.0 20.950 0 0.0 21.000 0 0.0 21.050 0 0.0 21.100 1 1.0 21.150 0 0.0 21.200 3 1.7 21.250 0 0.0 21.300 0 0.0 21.350 1 1.0 21.400 1 1.0 21.450 2 1.4 21.500 0 0.0 21.550 6 2.4 21.600 0 0.0 21.650 1 1.0 21.700 2 1.4 21.750 5 2.2 21.800 11 3.3 21.850 7 2.6 21.900 0 0.0 21.950 2 1.4 22.000 0 0.0 22.050 0 0.0 22.100 1 1.0 22.150 2 1.4 22.200 1 1.0 22.250 1 1.0 22.300 2 1.4 22.350 1 1.0 22.400 0 0.0 22.450 0 0.0 22.500 1 1.0 22.550 0 0.0 22.600 0 0.0 22.650 0 0.0 22.700 0 0.0 22.750 0 0.0 22.800 3 1.7 22.850 11 3.3 22.900 10 3.2 22.950 6 2.4 23.000 0 0.0 23.050 0 0.0 23.100 2 1.4 23.150 3 1.7 23.200 0 0.0 23.250 1 1.0 23.300 0 0.0 23.350 0 0.0 23.400 0 0.0 23.450 0 0.0 23.500 1 1.0 23.550 0 0.0 23.600 0 0.0 23.650 1 1.0 23.700 0 0.0 23.750 1 1.0 23.800 0 0.0 23.850 1 1.0 23.900 4 2.0 23.950 0 0.0 24.000 1 1.0 24.050 1 1.0 24.100 2 1.4 24.150 0 0.0 24.200 2 1.4 24.250 0 0.0 24.300 0 0.0 24.350 0 0.0 24.400 1 1.0 24.450 0 0.0 24.500 0 0.0 24.550 2 1.4 24.600 0 0.0 24.650 0 0.0 24.700 0 0.0 24.750 2 1.4 24.800 0 0.0 24.850 0 0.0 24.900 0 0.0 24.950 1 1.0 25.000 0 0.0 25.050 0 0.0 25.100 0 0.0 25.150 2 1.4 25.200 0 0.0 25.250 0 0.0 25.300 1 1.0 25.350 2 1.4 25.400 3 1.7 25.450 0 0.0 25.500 2 1.4 25.550 2 1.4 25.600 0 0.0 25.650 1 1.0 25.700 0 0.0 25.750 4 2.0 25.800 4 2.0 25.850 27 5.2 25.900 77 8.8 25.950 42 6.5 26.000 6 2.4 26.050 2 1.4 26.100 2 1.4 26.150 1 1.0 26.200 0 0.0 26.250 2 1.4 26.300 2 1.4 26.350 1 1.0 26.400 3 1.7 26.450 2 1.4 26.500 0 0.0 26.550 0 0.0 26.600 0 0.0 26.650 0 0.0 26.700 1 1.0 26.750 1 1.0 26.800 0 0.0 26.850 2 1.4 26.900 0 0.0 26.950 0 0.0 27.000 0 0.0 27.050 0 0.0 27.100 0 0.0 27.150 0 0.0 27.200 0 0.0 27.250 0 0.0 27.300 1 1.0 27.350 0 0.0 27.400 0 0.0 27.450 0 0.0 27.500 0 0.0 27.550 0 0.0 27.600 0 0.0 27.650 0 0.0 27.700 2 1.4 27.750 0 0.0 27.800 1 1.0 27.850 0 0.0 27.900 0 0.0 27.950 0 0.0 28.000 0 0.0 28.050 1 1.0 28.100 3 1.7 28.150 20 4.5 28.200 20 4.5 28.250 1 1.0 28.300 6 2.4 28.350 0 0.0 28.400 1 1.0 28.450 1 1.0 28.500 0 0.0 28.550 0 0.0 28.600 1 1.0 28.650 0 0.0 28.700 1 1.0 28.750 1 1.0 28.800 2 1.4 28.850 1 1.0 28.900 16 4.0 28.950 34 5.8 29.000 20 4.5 29.050 4 2.0 29.100 1 1.0 29.150 3 1.7 29.200 0 0.0 29.250 4 2.0 29.300 1 1.0 29.350 0 0.0 29.400 2 1.4 29.450 1 1.0 29.500 2 1.4 29.550 0 0.0 29.600 0 0.0 29.650 0 0.0 29.700 0 0.0 29.750 3 1.7 29.800 0 0.0 29.850 3 1.7 29.900 0 0.0 29.950 1 1.0 30.000 1 1.0 30.050 1 1.0 30.100 0 0.0 30.150 0 0.0 30.200 0 0.0 30.250 0 0.0 30.300 0 0.0 30.350 1 1.0 30.400 0 0.0 30.450 3 1.7 30.500 0 0.0 30.550 5 2.2 30.600 1 1.0 30.650 1 1.0 30.700 0 0.0 30.750 0 0.0 30.800 0 0.0 30.850 1 1.0 30.900 1 1.0 30.950 0 0.0 31.000 2 1.4 31.050 0 0.0 31.100 0 0.0 31.150 0 0.0 31.200 0 0.0 31.250 0 0.0 31.300 2 1.4 31.350 0 0.0 31.400 1 1.0 31.450 2 1.4 31.500 1 1.0 31.550 3 1.7 31.600 5 2.2 31.650 3 1.7 31.700 13 3.6 31.750 98 9.9 31.800 181 13.5 31.850 99 9.9 31.900 19 4.4 31.950 4 2.0 32.000 8 2.8 32.050 5 2.2 32.100 4 2.0 32.150 18 4.2 32.200 82 9.1 32.250 86 9.3 32.300 16 4.0 32.350 12 3.5 32.400 3 1.7 32.450 6 2.4 32.500 1 1.0 32.550 1 1.0 32.600 2 1.4 32.650 2 1.4 32.700 0 0.0 32.750 6 2.4 32.800 8 2.8 32.850 21 4.6 32.900 78 8.8 32.950 127 11.3 33.000 50 7.1 33.050 11 3.3 33.100 5 2.2 33.150 3 1.7 33.200 0 0.0 33.250 1 1.0 33.300 0 0.0 33.350 0 0.0 33.400 0 0.0 33.450 1 1.0 33.500 1 1.0 33.550 0 0.0 33.600 0 0.0 33.650 0 0.0 33.700 0 0.0 33.750 0 0.0 33.800 2 1.4 33.850 0 0.0 33.900 0 0.0 33.950 1 1.0 34.000 5 2.2 34.050 35 5.9 34.100 53 7.3 34.150 14 3.7 34.200 4 2.0 34.250 1 1.0 34.300 4 2.0 34.350 0 0.0 34.400 2 1.4 34.450 0 0.0 34.500 1 1.0 34.550 0 0.0 34.600 0 0.0 34.650 0 0.0 34.700 1 1.0 34.750 0 0.0 34.800 0 0.0 34.850 0 0.0 34.900 0 0.0 34.950 2 1.4 35.000 0 0.0 35.050 3 1.7 35.100 0 0.0 35.150 2 1.4 35.200 0 0.0 35.250 0 0.0 35.300 2 1.4 35.350 0 0.0 35.400 2 1.4 35.450 10 3.2 35.500 13 3.6 35.550 6 2.4 35.600 4 2.0 35.650 0 0.0 35.700 1 1.0 35.750 0 0.0 35.800 2 1.4 35.850 0 0.0 35.900 1 1.0 35.950 2 1.4 36.000 1 1.0 36.050 0 0.0 36.100 0 0.0 36.150 0 0.0 36.200 1 1.0 36.250 0 0.0 36.300 1 1.0 36.350 0 0.0 36.400 1 1.0 36.450 1 1.0 36.500 1 1.0 36.550 0 0.0 36.600 0 0.0 36.650 0 0.0 36.700 0 0.0 36.750 0 0.0 36.800 1 1.0 36.850 1 1.0 36.900 0 0.0 36.950 1 1.0 37.000 0 0.0 37.050 2 1.4 37.100 0 0.0 37.150 0 0.0 37.200 0 0.0 37.250 0 0.0 37.300 1 1.0 37.350 2 1.4 37.400 0 0.0 37.450 1 1.0 37.500 1 1.0 37.550 0 0.0 37.600 0 0.0 37.650 0 0.0 37.700 0 0.0 37.750 0 0.0 37.800 0 0.0 37.850 0 0.0 37.900 1 1.0 37.950 0 0.0 38.000 3 1.7 38.050 0 0.0 38.100 1 1.0 38.150 0 0.0 38.200 0 0.0 38.250 0 0.0 38.300 1 1.0 38.350 1 1.0 38.400 0 0.0 38.450 1 1.0 38.500 0 0.0 38.550 0 0.0 38.600 0 0.0 38.650 1 1.0 38.700 0 0.0 38.750 0 0.0 38.800 5 2.2 38.850 0 0.0 38.900 0 0.0 38.950 0 0.0 39.000 1 1.0 39.050 1 1.0 39.100 1 1.0 39.150 0 0.0 39.200 8 2.8 39.250 10 3.2 39.300 7 2.6 39.350 4 2.0 39.400 0 0.0 39.450 1 1.0 39.500 0 0.0 39.550 2 1.4 39.600 1 1.0 39.650 2 1.4 39.700 0 0.0 39.750 11 3.3 39.800 25 5.0 39.850 43 6.6 39.900 12 3.5 39.950 7 2.6 40.000 0 0.0 40.050 0 0.0 40.100 0 0.0 40.150 0 0.0 40.200 0 0.0 40.250 4 2.0 40.300 2 1.4 40.350 3 1.7 40.400 2 1.4 40.450 3 1.7 40.500 8 2.8 40.550 1 1.0 40.600 0 0.0 40.650 0 0.0 40.700 0 0.0 40.750 2 1.4 40.800 0 0.0 40.850 1 1.0 40.900 0 0.0 40.950 0 0.0 41.000 0 0.0 41.050 0 0.0 41.100 1 1.0 41.150 0 0.0 41.200 0 0.0 41.250 0 0.0 41.300 1 1.0 41.350 1 1.0 41.400 0 0.0 41.450 1 1.0 41.500 0 0.0 41.550 1 1.0 41.600 0 0.0 41.650 0 0.0 41.700 0 0.0 41.750 0 0.0 41.800 1 1.0 41.850 3 1.7 41.900 0 0.0 41.950 2 1.4 42.000 10 3.2 42.050 15 3.9 42.100 5 2.2 42.150 1 1.0 42.200 0 0.0 42.250 0 0.0 42.300 3 1.7 42.350 0 0.0 42.400 6 2.4 42.450 1 1.0 42.500 0 0.0 42.550 2 1.4 42.600 2 1.4 42.650 1 1.0 42.700 1 1.0 42.750 0 0.0 42.800 1 1.0 42.850 0 0.0 42.900 0 0.0 42.950 0 0.0 43.000 2 1.4 43.050 0 0.0 43.100 0 0.0 43.150 0 0.0 43.200 1 1.0 43.250 1 1.0 43.300 3 1.7 43.350 0 0.0 43.400 0 0.0 43.450 0 0.0 43.500 1 1.0 43.550 2 1.4 43.600 0 0.0 43.650 0 0.0 43.700 1 1.0 43.750 0 0.0 43.800 2 1.4 43.850 3 1.7 43.900 13 3.6 43.950 1 1.0 44.000 4 2.0 44.050 1 1.0 44.100 0 0.0 44.150 0 0.0 44.200 0 0.0 44.250 0 0.0 44.300 3 1.7 44.350 2 1.4 44.400 2 1.4 44.450 1 1.0 44.500 1 1.0 44.550 0 0.0 44.600 0 0.0 44.650 0 0.0 44.700 1 1.0 44.750 1 1.0 44.800 0 0.0 44.850 0 0.0 44.900 0 0.0 44.950 0 0.0 45.000 1 1.0 45.050 1 1.0 45.100 6 2.4 45.150 0 0.0 45.200 1 1.0 45.250 4 2.0 45.300 3 1.7 45.350 10 3.2 45.400 3 1.7 45.450 1 1.0 45.500 1 1.0 45.550 0 0.0 45.600 1 1.0 45.650 4 2.0 45.700 1 1.0 45.750 2 1.4 45.800 1 1.0 45.850 0 0.0 45.900 2 1.4 45.950 0 0.0 46.000 1 1.0 46.050 0 0.0 46.100 0 0.0 46.150 1 1.0 46.200 4 2.0 46.250 1 1.0 46.300 0 0.0 46.350 0 0.0 46.400 2 1.4 46.450 0 0.0 46.500 1 1.0 46.550 0 0.0 46.600 3 1.7 46.650 17 4.1 46.700 44 6.6 46.750 61 7.8 46.800 18 4.2 46.850 5 2.2 46.900 4 2.0 46.950 0 0.0 47.000 2 1.4 47.050 3 1.7 47.100 3 1.7 47.150 2 1.4 47.200 0 0.0 47.250 0 0.0 47.300 2 1.4 47.350 1 1.0 47.400 0 0.0 47.450 1 1.0 47.500 2 1.4 47.550 1 1.0 47.600 0 0.0 47.650 0 0.0 47.700 4 2.0 47.750 0 0.0 47.800 2 1.4 47.850 1 1.0 47.900 1 1.0 47.950 2 1.4 48.000 5 2.2 48.050 6 2.4 48.100 19 4.4 48.150 27 5.2 48.200 6 2.4 48.250 0 0.0 48.300 4 2.0 48.350 0 0.0 48.400 0 0.0 48.450 3 1.7 48.500 1 1.0 48.550 7 2.6 48.600 6 2.4 48.650 9 3.0 48.700 2 1.4 48.750 2 1.4 48.800 1 1.0 48.850 2 1.4 48.900 0 0.0 48.950 0 0.0 49.000 1 1.0 49.050 3 1.7 49.100 0 0.0 49.150 0 0.0 49.200 0 0.0 49.250 0 0.0 49.300 4 2.0 49.350 2 1.4 49.400 8 2.8 49.450 13 3.6 49.500 57 7.5 49.550 36 6.0 49.600 16 4.0 49.650 1 1.0 49.700 4 2.0 49.750 1 1.0 49.800 2 1.4 49.850 0 0.0 49.900 0 0.0 49.950 0 0.0 50.000 1 1.0 50.050 1 1.0 50.100 0 0.0 50.150 3 1.7 50.200 0 0.0 50.250 1 1.0 50.300 1 1.0 50.350 3 1.7 50.400 1 1.0 50.450 9 3.0 50.500 35 5.9 50.550 26 5.1 50.600 5 2.2 50.650 5 2.2 50.700 3 1.7 50.750 1 1.0 50.800 1 1.0 50.850 0 0.0 50.900 1 1.0 50.950 0 0.0 51.000 2 1.4 51.050 1 1.0 51.100 1 1.0 51.150 2 1.4 51.200 6 2.4 51.250 13 3.6 51.300 22 4.7 51.350 14 3.7 51.400 3 1.7 51.450 2 1.4 51.500 0 0.0 51.550 0 0.0 51.600 0 0.0 51.650 3 1.7 51.700 0 0.0 51.750 1 1.0 51.800 0 0.0 51.850 1 1.0 51.900 1 1.0 51.950 0 0.0 52.000 3 1.7 52.050 9 3.0 52.100 28 5.3 52.150 20 4.5 52.200 7 2.6 52.250 1 1.0 52.300 1 1.0 52.350 2 1.4 52.400 1 1.0 52.450 0 0.0 52.500 2 1.4 52.550 0 0.0 52.600 1 1.0 52.650 1 1.0 52.700 0 0.0 52.750 1 1.0 52.800 0 0.0 52.850 0 0.0 52.900 0 0.0 52.950 0 0.0 53.000 0 0.0 53.050 1 1.0 53.100 2 1.4 53.150 12 3.5 53.200 29 5.4 53.250 22 4.7 53.300 12 3.5 53.350 1 1.0 53.400 1 1.0 53.450 1 1.0 53.500 0 0.0 53.550 0 0.0 53.600 0 0.0 53.650 1 1.0 53.700 1 1.0 53.750 1 1.0 53.800 0 0.0 53.850 0 0.0 53.900 3 1.7 53.950 0 0.0 54.000 0 0.0 54.050 0 0.0 54.100 0 0.0 54.150 1 1.0 54.200 0 0.0 54.250 0 0.0 54.300 0 0.0 54.350 0 0.0 54.400 3 1.7 54.450 1 1.0 54.500 3 1.7 54.550 1 1.0 54.600 2 1.4 54.650 2 1.4 54.700 0 0.0 54.750 0 0.0 54.800 0 0.0 54.850 0 0.0 54.900 2 1.4 54.950 0 0.0 55.000 0 0.0