| 2q | I (obs) |
|---|---|
| 7.5 | 67 |
| 8.07 | 7727 |
| 10.25 | 3634 |
| 11.77 | 104 |
| 14.82 | 1731 |
| 15.05 | 557 |
| 16.09 | 199 |
| 16.64 | 108 |
| 16.9 | 448 |
| 17.15 | 1861 |
| 18.07 | 740 |
| 18.27 | 185 |
| 18.81 | 2587 |
| 19.36 | 1031 |
| 20.63 | 680 |
| 20.84 | 65 |
| 22.67 | 228 |
| 23.45 | 626 |
| 24.27 | 1793 |
| 24.41 | 135 |
a = 23.742 Å, b = 6.176 Å, c =
11.035 Å
a = 90°, b = 97.88°, g = 90°
Crystal system is monoclinic as a¹b¹c and a=g = 90°, b¹90°
2. Bravais lattice type will be mP because the crystal system is monoclinic and the lattice type is type is primitive.
3. From hkl program space group is P2/m which does not have screw axes or glide planes therefore there are no reflection conditions.
4. Space group is P2/m.
5.
| 2q | h | k | l | 2q | h | k | l | 2q | h | k | l | ||
| 7.50 | 2 | 0 | 0 | 14.82 | 1 | 1 | 0 | 16.90 | -2 | 0 | 2 | ||
| 8.07 | 0 | 0 | 1 | 15.05 | 4 | 0 | 0 | 17.15 | 1 | 1 | 1 | ||
| 10.25 | -2 | 0 | 1 | 16.09 | -4 | 0 | 1 | 18.07 | 4 | 0 | 1 | ||
| 11.77 | 2 | 0 | 1 | 16.64 | -1 | 1 | 1 | 18.27 | 3 | 1 | 0 |
| a (Å) | b (Å) | c (Å) | a (°) | b (°) | g (°) | |
| Value | 23.72951 | 6.17132 | 11.03174 | 89.9869 | 97.9013 | 90.0200 |
| ESD | 0.00928 | 0.00333 | 0.00518 | 0.0461 | 0.0176 | 0.0350 |
2qzero = -0.0135 ± 0.0053
The peaks are very weak in the high angle region so cannot include the high angle data and greater error is caused at high angles by the the diffractometer as collecting data.