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Cell parameters : a = 6.94802(7) Å,   b = 8.46618(8) Å,   c = 5.38904(6) Å
Cell volume,V (Å3) : 317.00

Atom x y z B(iso)
Pb   0.1671(1)   0.1879(1) 1/4 -
S 0.1848(3) 0.4358(2) 3/4 0.93(4)
O(1) 0.0958(2) 0.5907(1) 3/4 -
O(2) 0.0429(2) 0.3068(2) 3/4 -
O(3) 0.3082(1) 0.4192(1) 0.9727(1) -

Atom  B11 B22 B33 B23 B31 B12
Pb    1.58(4)    1.19(3) 2.22(4) 0 0 0.20(4)
O(1) 2.11(6) 1.43(6) 2.95(7) 0 0 0.81(4)
O(2) 1.54(6) 1.73(6) 2.24(7) 0 0 -0.77(5)  
O(3) 1.60(4) 1.77(4) 1.36(4) 0.07(3) -0.40(3)   -0.18(4)  

Instrumental : U = 0.175(2)°2,   V = -0.460(5)°2,   W = 0.448(3)°2,   h = 0.262(3)

Structural Parameters :

Bonds LengthsValue   Bonds AnglesValue
S-O(1)1.450(2) Å   Ð O(1)-S-O(2)112.7(2)°
S-O(2)1.471(3) Å   Ð O(1)-S-O(3)109.4(2)°
S-O(3)1.482(2) Å   Ð O(1)-S-O(3)¢ 109.4(2)°
S-O(3)¢ 1.482(2) Å   Ð O(2)-S-O(3)108.5(1)°
    Ð O(2)-S-O(3)¢ 108.5(1)°
    Ð O(3)-S-O(3)¢ 108.2(2)°
The " ¢ " indicates that the coordinates of this atom are symmetry related (by a mirror plane in this instance) to the coordinates of a refined atom with the same name. (Note that the bond lengths calculated here are uncorrected for thermal effects, e.g. molecular libration.)